{"id":20867,"date":"2024-06-17T19:20:09","date_gmt":"2024-06-18T03:20:09","guid":{"rendered":"https:\/\/integratechem.com\/plastificante-de-citrato-de-tributilo-de-gran-pureza\/"},"modified":"2026-04-02T06:51:41","modified_gmt":"2026-04-02T14:51:41","slug":"high-purity-tributyl-citrate-plasticizer","status":"publish","type":"post","link":"https:\/\/integratechem.com\/es\/high-purity-tributyl-citrate-plasticizer\/","title":{"rendered":"Plastificante de citrato de tributilo de gran pureza"},"content":{"rendered":"\n

1. Qu\u00e9 es el plastificante de citrato de tributilo de gran pureza<\/h2><\/div>\n\n

El plastificante de citrato de tributilo de alta pureza es un \u00e9ster de \u00e1cido c\u00edtrico de n-butanol, un l\u00edquido aceitoso incoloro que es soluble en la mayor\u00eda de disolventes org\u00e1nicos. Es un plastificante no t\u00f3xico que suministran los proveedores de China. Los fabricantes y las f\u00e1bricas de China lo utilizan para granular PVC no t\u00f3xico y fabricar materiales de envasado de alimentos. <\/p>\n\n

\"Plastificante<\/figure><\/div>\n\n

2. Qu\u00e9 propiedades tiene<\/h2><\/div>\n\n

Como \u00e9ster de \u00e1cido carbox\u00edlico del alcohol graso, los fabricantes y proveedores consideran que pertenece a un derivado del \u00e1cido carbox\u00edlico y contiene un grupo carbonilo. Por tanto, el plastificante de citrato de tributilo de alta pureza es un compuesto polar con un punto de ebullici\u00f3n m\u00e1s bajo que el \u00e1cido y el alcohol correspondientes. Y es similar a los aldeh\u00eddos o cetonas con el mismo n\u00famero de \u00e1tomos de carbono. Es vol\u00e1til y tiene fragancia. <\/p>\n\n

Factoies y fabricantes pueden hacer que el \u00e9ster de \u00e1cido c\u00edtrico reaccione con el agua para producir \u00e1cido c\u00edtrico y n-butanol. Su capacidad de hidr\u00f3lisis es menor que la de los halogenuros de acilo y los anh\u00eddridos, pero mayor que la de las amidas. Los proveedores y fabricantes de China consideran estas reacciones como la sustituci\u00f3n del H de la mol\u00e9cula HOH por grupos acilo. Los halogenuros de acilo y los anh\u00eddridos tienen la mayor capacidad de acilaci\u00f3n, por lo que las f\u00e1bricas y los fabricantes suelen utilizarlos como agentes acilantes en la s\u00edntesis org\u00e1nica. <\/p>\n\n

Los proveedores de China llaman saponificaci\u00f3n a la hidr\u00f3lisis de \u00e9steres en soluci\u00f3n alcalina, porque las sales de \u00e1cidos grasos superiores obtenidas por hidr\u00f3lisis alcalina de aceites y grasas son jabones.<\/p>\n\n

Cuando los \u00e9steres reaccionan con los alcoholes bajo la cat\u00e1lisis del \u00e1cido clorh\u00eddrico o del alcohol s\u00f3dico, entonces generamos otro alcohol y un \u00e9ster. A esta reacci\u00f3n la llamamos transesterificaci\u00f3n. Tambi\u00e9n es reversible. Por ejemplo, el citrato de trietilo reacciona con el n-butanol para generar citrato de tributilo y etanol. <\/p>\n\n

Los \u00e9steres de \u00e1cidos grasos pueden reaccionar con el amon\u00edaco para generar amidas. Por ejemplo, el citrato<\/a> de trib<\/a> utilo (TBC)<\/a> se acetila para generar citrato de tributilo acetilado (ATBC)<\/a>. <\/p>\n\n

El citrato de tributilo de gran pureza puede reaccionar con reactivos de Grignard para generar alcoholes terciarios.<\/p>\n\n

El acetil tributil citrato<\/a> es m\u00e1s f\u00e1cil de reducir que los \u00e1cidos carbox\u00edlicos. En s\u00edntesis, los \u00e1cidos carbox\u00edlicos suelen reducirse a alcoholes mediante \u00e9steres. El agente reductor m\u00e1s utilizado es el sodio m\u00e1s etanol. Los alcoholes resultantes son el alcohol utilizado en la esterificaci\u00f3n original o el alcohol primario generado por la reducci\u00f3n del grupo acilo. <\/p>\n\n

3. Cu\u00e1l es su mecanismo de reacci\u00f3n<\/h2><\/div>\n\n

La gente calienta \u00e1cido c\u00edtrico y n-butanol en presencia de una peque\u00f1a cantidad de catalizador \u00e1cido para generar un plastificante de citrato de tributilo de gran pureza. El catalizador es cloruro de hidr\u00f3geno seco y una resina de intercambio i\u00f3nico de \u00e1cido fuerte. Tambi\u00e9n las f\u00e1bricas utilizan \u00e1cido sulf\u00farico concentrado. Llamamos a esta reacci\u00f3n esterificaci\u00f3n. Cuando la esterificaci\u00f3n genera citrato de tributilo, hay dos v\u00edas posibles para la deshidrataci\u00f3n de las mol\u00e9culas de \u00e1cido c\u00edtrico y n-butanol. Los estudios han demostrado que la ruptura del enlace qu\u00edmico se produce entre el grupo acilo y el ox\u00edgeno. Es decir, el agua generada durante la reacci\u00f3n procede del grupo hidroxilo del \u00e1cido c\u00edtrico y del enlace de hidr\u00f3geno del n-butanol. <\/p>\n\n

La esterificaci\u00f3n es una reacci\u00f3n reversible. Cuando se produce el equilibrio, hay un n\u00famero determinado de reactivos y productos. Por ejemplo, cuando el mismo 1 mol de \u00e1cido c\u00edtrico y 3 moles de n-butanol reaccionan en presencia de una peque\u00f1a cantidad de \u00e1cido sulf\u00farico, al producirse el equilibrio, parte del \u00e1cido c\u00edtrico y del n-butanol se convierten en plastificante de citrato de tributilo de gran pureza. El calentamiento y la adici\u00f3n de catalizadores s\u00f3lo pueden acelerar la velocidad de reacci\u00f3n, pero no tienen ning\u00fan efecto sobre la composici\u00f3n del material de equilibrio. <\/p>\n\n

4. C\u00f3mo mejorar la producci\u00f3n y el rendimiento del plastificante de citrato de tributilo de gran pureza<\/h2><\/div>\n\n

Para mejorar el rendimiento, las f\u00e1bricas suelen a\u00f1adir \u00e1cido c\u00edtrico o n-butanol en exceso. O eliminan el agua generada de la mezcla de reacci\u00f3n. Si el punto de ebullici\u00f3n del \u00e9ster generado es muy bajo, los fabricantes y proveedores de China pueden hacer que el \u00e9ster se evapore. Sin embargo, el punto de ebullici\u00f3n del citrato de tributilo es de 150\u00b0C, as\u00ed que primero evaporamos el agua. En resumen, se destru\u00eda el equilibrio para aumentar el rendimiento. En la producci\u00f3n industrial, utilizamos \u00e1cido c\u00edtrico en exceso para evaporar la mezcla de ebullici\u00f3n constante de plastificante de citrato de tributilo de gran pureza y agua. Y luego la gente a\u00f1ad\u00eda continuamente \u00e1cido c\u00edtrico y butanol para evaporar el citrato de tributilo y el agua para la producci\u00f3n continua. <\/p>\n\n

5. Aplicaci\u00f3n del plastificante de citrato de tributilo de gran pureza<\/h2><\/div>\n\n

Los \u00e9steres de citrato pueden reaccionar con amon\u00edaco para formar amida. El citrato de tributilo se acetila para formar el n\u00ba CAS 77 90 7 citrato de tributilo acetilado. <\/p>\n\n

El citrato de tributilo (TBC) es un l\u00edquido aceitoso incoloro, soluble en la mayor\u00eda de disolventes org\u00e1nicos. Y tiene baja volatilidad, alta eficacia plastificante y es f\u00e1cilmente soluble en resina. Puede aumentar la resistencia a las bajas temperaturas, la resistencia al agua y la resistencia al moho del producto. El citrato de tributilo es un plastificante no t\u00f3xico que las f\u00e1bricas utilizan como plastificante en la granulaci\u00f3n de PVC no t\u00f3xico. Tambi\u00e9n se utiliza en envases de alimentos, juguetes infantiles, suministros m\u00e9dicos, cloruro de polivinilo y producci\u00f3n de copol\u00edmeros de cloruro de vinilo. <\/p>\n\n

6. Reacci\u00f3n de hidr\u00f3lisis del plastificante de citrato de tributilo de gran pureza<\/h2><\/div>\n\n

Todos los \u00e9steres se hidrolizan m\u00e1s f\u00e1cilmente en soluciones \u00e1cidas o alcalinas que en soluciones neutras. Como las soluciones \u00e1cidas aportan iones de hidr\u00f3geno, pueden combinarse con el ox\u00edgeno carbon\u00edlico polar para hacer que el ox\u00edgeno tenga carga positiva. As\u00ed, la nube de electrones \u03c0 se transfiere m\u00e1s al ox\u00edgeno. Esto hace que el carbono carbonilo est\u00e9 cargado positivamente y sea m\u00e1s propenso a las reacciones de adici\u00f3n nucleof\u00edlica. Incluso los nucle\u00f3filos m\u00e1s d\u00e9biles, como el agua, pueden sufrir reacciones de adici\u00f3n nucleof\u00edlica. Sin el efecto catalizador del \u00e1cido, la velocidad de hidr\u00f3lisis de los \u00e9steres es muy lenta. Los fabricantes y las f\u00e1bricas deben calentar y a\u00f1adir un catalizador para la reacci\u00f3n de hidr\u00f3lisis de los \u00e9steres. <\/p>\n\n

La reacci\u00f3n de hidr\u00f3lisis de los \u00e9steres es una reacci\u00f3n reversible, y se puede completar la reacci\u00f3n en presencia de una gran cantidad de agua. Los \u00e9steres equimolares y el agua forman una mezcla equilibrada en soluciones \u00e1cidas o neutras, mientras que en soluciones alcalinas, como los iones hidr\u00f3xido son nucle\u00f3filos fuertes, una vez generados los \u00e1cidos carbox\u00edlicos, forman inmediatamente sales con los \u00e1lcalis, destruyendo el equilibrio y permitiendo que la reacci\u00f3n de hidr\u00f3lisis llegue hasta el final. <\/p>\n\n

7. C\u00f3mo garantizar la calidad del producto Plastificante de citrato de tributilo de gran pureza<\/h2><\/div>\n\n

Nuestra f\u00e1brica cuenta con equipos de producci\u00f3n avanzados, tecnolog\u00eda de producci\u00f3n madura, instrumentos de prueba completos y m\u00e9todos de an\u00e1lisis estandarizados, y adopta el proceso de producci\u00f3n de esterificaci\u00f3n continua, separaci\u00f3n por destilaci\u00f3n, neutralizaci\u00f3n y lavado con agua, de modo que el contenido de \u00e1cido libre y agua en el producto es bajo. Por lo tanto, el producto tiene un alto contenido, un bajo valor \u00e1cido y contenido de agua, no es f\u00e1cil de hidrolizar y tiene una calidad estable. Esto goza de gran reconocimiento entre los clientes nacionales y extranjeros. <\/p>\n\n

Hot Tags: proveedores China, fabricantes, f\u00e1brica, n\u00ba CAS 77-94-1<\/a>, Plastificante no t\u00f3xico<\/a>, Plastificante para resinas celul\u00f3sicas<\/a>, Plastificante para PVC<\/a>, \u00c9ster tribut\u00edlico<\/a><\/p>\n\n

Enlaces relacionados: N\u00ba CAS 77 89 4<\/a>, N\u00ba CAS 77 90 7<\/a>, N\u00ba CAS 77 93 0<\/a>, N\u00ba CAS 77 94 1<\/a>, Citrato de tributilo<\/a> (TBC)<\/a>, Plastificante de alta calidad Citrato de tributilo TBC<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"

1. 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